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Gas chromatographic - Mass spectrometric cardiotonic glycosides detection in equine urine doping analysis

dc.creatorKiousi, P.en
dc.creatorAngelis, Y. S.en
dc.creatorKoupparis, M.en
dc.creatorKouretas, D.en
dc.creatorDiakakis, N.en
dc.creatorDesiris, A.en
dc.creatorGeorgakopoulos, C. G.en
dc.date.accessioned2015-11-23T10:34:51Z
dc.date.available2015-11-23T10:34:51Z
dc.date.issued2004
dc.identifier10.1365/s10337-004-0214-z
dc.identifier.issn0009-5893
dc.identifier.urihttp://hdl.handle.net/11615/29423
dc.description.abstractA screening method for the detection of cardiotonic glycosides in horse's urine is presented in this paper. This method is based on the detection by gas chromatography-mass spectrometry (GC-MS) and gas chromatography-high resolution mass spectrometry (GC-HRMS) of the trimethylsilyl (TMS) derivatives of the aglycon moieties of these compounds after solid phase extraction and methanolysis, according to the standard procedure currently used for the screening of anabolic steroids in horses, in the Athens Doping Control Laboratory. This validated method was also applied for the excretion study of digoxin in two mare horses after a single administration of a 75 mug Kg(-1) oral dose, by GC-MS and GC-HRMS.en
dc.source.uri<Go to ISI>://WOS:000224155600014
dc.subjectgas chromatography - mass spectrometryen
dc.subjectsolid phase extractionen
dc.subjectcardiotonic glycosidesen
dc.subjectdoping drugsen
dc.subjectdigoxinen
dc.subjectequine urineen
dc.subjectLIQUID-CHROMATOGRAPHYen
dc.subjectCARDIAC-GLYCOSIDESen
dc.subjectDIGOXINen
dc.subjectPLASMAen
dc.subjectASSAYen
dc.subjectHORSEen
dc.subjectBiochemical Research Methodsen
dc.subjectChemistry, Analyticalen
dc.titleGas chromatographic - Mass spectrometric cardiotonic glycosides detection in equine urine doping analysisen
dc.typejournalArticleen


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